http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103289087-B
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08G73-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D413-14 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D413-10 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D413-06 |
filingDate | 2013-04-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2015-10-14-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2015-10-14-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-103289087-B |
titleOfInvention | A kind of preparation method of benzoxazine-epoxy resin |
abstract | The invention discloses a kind of preparation method of benzoxazine-epoxy resin, it is characterized in that: aminated compounds, solvent, formalin are joined in reactor, 0 ~ 30 DEG C of stirring reaction 1 ~ 2 hour, add phenolic compound, 85 ~ 95 DEG C of back flow reaction 2 ~ 4 hours, again catalyzer and alkaline phosphatase hydrogen disalt are added, under agitation add part aqueous hydrogen peroxide solution, stirring reaction is after 1 ~ 2 hour, add remaining aqueous hydrogen peroxide solution again, at 60 ~ 90 DEG C, react 3 ~ 16 hours again; Be cooled to room temperature, leave standstill 2 ~ 8 hours, the organic phase isolating top is benzoxazine-epoxy resin product.Present method adopts the benzoxazine resin of an autoclave interfacial synthesis method anamorphic zone epoxide group, concise in technology, and cost is low; Obtained benzoxazine-epoxy resin can be widely used in the field such as glass fibre fabric swatch (pipe), glasscloth preimpregnation material identical with common epoxy or resol. |
priorityDate | 2013-04-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 93.