http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103265557-A
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_735eae3153d0363cf9a50ec8a838ea2c |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D493-10 |
filingDate | 2013-05-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_944d74dfd7acdc3f114494a666b327d6 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_bfcd4569e9c6acb4b68eae5d3126fbbd |
publicationDate | 2013-08-28-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-103265557-A |
titleOfInvention | Technology for separating and preparing high-purity ailanthone |
abstract | The invention relates to a technology for separating and preparing high-purity ailanthone. The technology comprises the following detailed steps of: grinding ailanthus tree bark taken as raw material; adding 75-90% ethanol to implement ultrasonic extraction, wherein the amount of the ethyl alcohol is 6-12 times that of the ground bark; adding an appropriate amount of kieselguhr into an extracted solution, preserving heat and destaining; concentrating a destained solution, enriching the destained solution by a polyamide resin column; eluting the destained solution by an 80% ethanol solution; and concentrating an eluent, implementing drying, and separating dried products in a high-speed counter-current chromatography way, thus obtaining the ailanthone. The method is simple and convenient to operate, high in separation efficiency, good in product purity, and suitable for industrial production. |
isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-108948037-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-111620888-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-112314612-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-112730676-A |
priorityDate | 2013-05-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 33.