http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103265489-B

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_b52440d7e97d4de5d808147356f12e96
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D221-28
filingDate 2013-06-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2015-03-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b0046d4cae69c848ae4b4bff71daf342
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0579e26620c4a20679b66f6f73ee42a3
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a656b561e595ec6f8f92962fc12578ab
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_fed80d8e40d21911ebe61355e6824158
publicationDate 2015-03-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-103265489-B
titleOfInvention Preparation method of ent-(14S)-3-methoxyl-17-morphinan
abstract The invention discloses a preparation method of ent-(14S)-3-methoxyl-17-morphinan. The method comprises the following step of: enabling (+)-N-methyl-1-(4- methoxyl) benzyl-1,2,3,4,5,6,7,8-octahydro isoquinoline (I) to be subjected to cyclization reaction under the action of lewis acid, so as to produce the high-purity ent-(14S)-3-methoxyl-17-morphinan (D). The preparation method is simple in process, the prepared product is high in purity, and in comparison with the standard substance, the purity of the product is completely consistent with that of the standard substance.
priorityDate 2013-06-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 31.