http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103254229-B

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Predicate Object
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F9-40
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07B59-00
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F9-113
filingDate 2013-05-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2016-06-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2016-06-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-103254229-B
titleOfInvention A kind of deuterium-labeled organic phosphorous insecticide synthetic method of stable isotope
abstract The present invention relates to a kind of deuterium-labeled organic phosphorous insecticide synthetic method of stable isotope, the method utilizes stable isotope deuterium-labeled or natural abundance methyl alcohol and phosphorus trichloride reaction to generate the deuterium-labeled dimethylphosphite of stable isotope or trimethyl phosphite, then trichoro-aldehyde that is deuterium-labeled with stable isotope or natural abundance is obtained by reacting the deuterium-labeled organic phosphorous insecticide of stable isotope. Compared with prior art, cold labeling Trichlorphon that the present invention obtains or SD-1750, after separation is purified, chemical purity reaches more than 98.0%, and isotopic abundance, at more than 98.0%atomD, can fully meet the demand of field of food safety residue detection.
priorityDate 2013-05-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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