http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103196982-B

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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N27-447
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N1-34
filingDate 2013-04-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2014-08-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_9d2807b529db0446286df44b0de41856
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_c40702b3fc2daaecf19cb93cc6fba052
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_1614329011eb0642176d018a7ce3b3e2
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http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_1c04411070604a7b2e59f9e91a897991
publicationDate 2014-08-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-103196982-B
titleOfInvention Method for determining content of pyrroloquinoline quinone in biological sample by magnetic solid-phase extraction-capillary zone electrophoresis
abstract The invention provides a method for determining the content of pyrroloquinoline quinone in a biological sample by magnetic solid-phase extraction-capillary zone electrophoresis and belongs to the field of a life analyzing technology. According to the method disclosed by the invention, SiO2 and adsorbents with different polarities are mixed; and the adsorbents have different selective properties on compounds with different hydrophobic properties, so that the effective separation can be carried out. A capillary electrophoresis method adopted by the invention adds a modifying agent beta-cyclodextrin; trifluoroacetic acid is firstly added into a capillary electrophoresis buffering system to solve the trailing problem of a peak in a capillary electrophoresis picture; and the symmetrical property of the peak is obviously better than that of a document report. The method disclosed by the invention is rapid and convenient, and can be used for determining the content of the PQQ in milk by utilizing a magnetic solid-phase extraction technology being combined with capillary electrophoresis firstly. Compared with a document method, the method disclosed by the invention improves the separation efficiency by 6 times.
priorityDate 2013-04-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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