http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103193606-B
Outgoing Links
| Predicate | Object |
|---|---|
| assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_226fa86f9790e799a44846e2f6319e98 |
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C39-38 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C39-27 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C39-28 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C43-23 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C41-22 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C37-62 |
| filingDate | 2013-04-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| grantDate | 2015-04-08-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a1e9a8c01ff0d4ada89ed43afbc71831 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_397f4fa8f7475e5ac28327174bcd478a http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_bfc55d100fd8f27be4e0b4aa26f2f83d |
| publicationDate | 2015-04-08-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-103193606-B |
| titleOfInvention | Synthesis method of brominated phenolic compound |
| abstract | The invention relates to a synthesis method of a brominated phenolic compound, belonging to the technical field of organic synthesis and solving the problems of the existing synthesis method of brominated phenolic compound, such as bad environmental protection property and low reaction efficiency. The synthesis method comprises the steps of: adding a phenol derivative, terpyridyl ruthenium chloride, sodium persulfate, a metal bromide and an organic solvent in a reaction container, stirring the mixture at room temperature under the condition of visible light irradiation to react to obtain reaction liquid, separating and purifying the reaction liquid to obtain the brominated phenolic compound. The synthesis method provided by the invention is simple to operate, a small dose of photocatalyst is used and can be recycled, the selected brominating agent and oxidant are low-toxic and even non-toxic, the reaction yield is high, environmentally-friendly, clean and facile visible light is used for irradiation during reaction, and a common filament lamp, an LED lamp or sunlight is used as a light source. The synthesis method provided by the invention is mainly used for synthesizing brominated phenolic compounds. |
| priorityDate | 2013-04-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 68.