http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103172480-B
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_550246a1a90f3c3034cf90d3392188d9 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C41-22 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C43-225 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07B39-00 |
filingDate | 2013-03-05-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2015-01-21-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b64a1787a8d2ed8cd1075dff0675a741 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_94f8798f337f5568b26a93146f5c0340 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a88420a88b7902de0ecc28ef525948f0 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4a12dca243b50b227e1458a40a3d2239 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6186e7d89da8565d84f5f5f822eca5e2 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4f9e87eb7d18fa4ae32175ed56c12db2 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2e668c2619d4d4bc9a8605b5d5645856 |
publicationDate | 2015-01-21-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-103172480-B |
titleOfInvention | Method for preparing iodo aromatic hydrocarbon |
abstract | The invention relates to a method for preparing iodo aromatic hydrocarbon. According to the invention, an aromatic-ring-containing compound, I2, a catalyst NO2, and an organic solvent are added into a reaction vessel, wherein a substance amount ratio of the aromatic-ring-containing compound to I2 to the catalyst NO2 is 1:0.2-3:0.01-5; the reaction vessel is sealed; the mixture is subjected to a reaction for 5min-40h under stirring and under a temperature of 10-180 DEG C; after the reaction, the product is cooled to room temperature; the mixture after the reaction is purified through column chromatography, such that iodo aromatic hydrocarbon is obtained. According to the iodo aromatic hydrocarbon preparation method, the adopted raw materials and reagents have the advantages of simple components and low cost, such that production cost is substantially reduced. Acid is not used, a low-boiling-point solvent is selected, the product is easy to separate and purify, the product has high purity, and the process is simple. |
priorityDate | 2013-03-05-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 79.