http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103130237-B
Outgoing Links
Predicate | Object |
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classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/Y02P20-52 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01B37-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/B01J35-023 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01B39-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01B39-40 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/B01J6-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D201-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/B01J29-40 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01B39-02 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D201-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01B39-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D223-10 |
filingDate | 2012-11-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2016-08-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2016-08-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-103130237-B |
titleOfInvention | For preparing the method for zeolite mechanograph and for the method preparing epsilon-caprolactams |
abstract | The present invention is provided to prepare the method for zeolite mechanograph and for the method preparing ε caprolactam, described zeolite mechanograph has outstanding mechanical strength.The method being used for preparing zeolite mechanograph according to the present invention comprises the following steps (1) to (5): (1) carries out hydrothermal synthesis reaction to the mixture containing silicon compound, water and quaternary ammonium hydroxide;(2) reactant mixture containing crystallization obtained in filtration step (1), to be separated into the concentrate containing crystallization and filtrate;(3) concentrate containing crystallization obtained in step (2) is washed with water, until the washed solution obtained by washing becomes 8.5 to 9.5 at the pH of 25 DEG C;(4) crystallization obtained in molding process (3);(5) mechanograph obtained in calcining step (4).By using the zeolite mechanograph prepared by this method as catalyst, prepare ε caprolactam by cyclohexanone-oxime Beckmann rearrangement in the gas phase. |
priorityDate | 2011-11-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 71.