| Predicate |
Object |
| assignee |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_48df6bc4ebf937c660e36d97dec66663 |
| classificationIPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D263-58
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C09K11-06 |
| filingDate |
2013-02-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| grantDate |
2015-02-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| inventor |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8ec0e12a194b2a779a956a865c1e1f96
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_65531350a0f342987c0f0f554277f344
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_af4996c97e7e9da9ce1e986d8714afa5
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_945d403363e2eed4bdc8aec41ede0b85
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4ef80a4608920378ee41c2f25fedcd38
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6ef7b1ebda04685498b8766690050321
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_59e3f15b70036d273aba383c3a7b23cc
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d24ba70d49e09008706908af4c580334 |
| publicationDate |
2015-02-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber |
CN-103113321-B |
| titleOfInvention |
2-(methylmercapto) benzo [d] oxazole-5-carboxylic acid and preparation method thereof |
| abstract |
The invention discloses a preparation method of a 2-(methylmercapto) benzo [d] oxazole-5-carboxylic acid. The preparation method comprises the following steps: (1) synthesizing 3-nitro-4-hydroxybenzoate; (2) synthesizing 3-amino-4-hydroxybenzoic acid; (3) synthesizing 2-sulfydryl benzo [d] oxazole-5-carboxylic acid; and (4) synthesizing the 2-(methylmercapto) benzo [d] oxazole-5-carboxylic acid; and as the test result shows, the electrogenerated chemiluminescence performance of the 2-(methylmercapto) benzo [d] oxazole-5-carboxylic acid is stable within the potential range of (-2 to 0)V; and the luminescent intensity in a water phase is obviously higher than that in an organic phase. |
| priorityDate |
2013-02-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type |
http://data.epo.org/linked-data/def/patent/Publication |