http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103086842-B
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_e3041781d58f04095650f62530800996 http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_641a820a6d43ebb43841f505cae934ba http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_f9ff27001608a152d4ca5b1ab5789e6d http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_36cf6e45f657a14dff8ac02dff6d556b http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_bb4c8c9f4f1f566965d5861055385538 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C17-263 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C25-18 |
filingDate | 2013-02-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2015-04-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_10f578d1fd5b97b1cd630cc00324ca7a http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3c42ec82426d91b9b020f36900a9f104 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_989c8d91656425caa2e6f52e9645c768 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_85973004e440a2f785b24f98309da7be http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2429f8337c15d0ee336ba87aab686e0b |
publicationDate | 2015-04-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-103086842-B |
titleOfInvention | Synthesis method of 3,3',4,4',5,5'-hexafluorobiphenyl |
abstract | The invention discloses a synthesis method of 3,3',4,4',5,5'-hexafluorobiphenyl. The synthesis method of 3,3',4,4',5,5'-hexafluorobiphenyl comprises the following step: performing Suzuki coupling reaction on 3,4,5-trifluorohalogenobenzene of Formula 1 and 3,4,5-trifluorobenzene boride of Formula 2 under the action of a palladium catalyst in the presence of an organic phosphine ligand, an additive and alkali in solvent, wherein X is chlorine, bromine or iodine, y is 1 or 2, OR is hydroxyl, or groups shown in the specification, C2-6 represents alkylidene, and C1-6 represents alkyl; when y is 1, OR is a group shown in the specification; when y is 2, OR is hydroxyl or a group shown in the specification; and the additive is a salt which has a general formula MnAm, wherein M is ammonium, lithium, sodium, potassium, iron or manganese, A is fluorine, chlorine, bromine, iodine, sulfate or acetate, n is 1 or 2, and m is 1, 2 or 3. |
priorityDate | 2013-02-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 147.