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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D275-04
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D275-04
filingDate 2011-12-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2016-04-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2016-04-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-103073518-B
titleOfInvention The method of preparation 1,2-benzisothiazole-2-ketone and salt thereof
abstract The present invention relates to the method for preparation 1,2-benzisothiazole-2-ketone and salt thereof.The method comprises: by being heated together with METHYLPYRROLIDONE by sodium sulphite hydrate, and sodium sulphite hydrate is dewatered at least partly; 2-chlorobenzamide is added in gained mixture, heats further; By gained mixture cooling also use hydrogen peroxide treatment.The method obtains the sodium salt of 1,2-benzisothiazole-2-ketone with good yield.If needed, 1, the 2-benzisothiazole-2-ketone dissociated can be obtained by acidifying.
priorityDate 2011-10-26-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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