http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102992391-B
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_090e02c1ea64ae911504a83ff1588d71 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B82Y40-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01G3-12 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01G21-21 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01G11-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01G45-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01G9-08 |
filingDate | 2012-09-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2014-04-23-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a222fa9aaa908ba65957a991adf2f572 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_96b558d52d41c2be7c4aa7c01f986334 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_423b57186263ee15e2053596226c6aae http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_81d3f10653876585d01cb73021c25f15 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_c6cbab166a0fcd8d6708efc17ca0b477 |
publicationDate | 2014-04-23-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-102992391-B |
titleOfInvention | Method and device for preparing nano metal sulfide powder by using continuous flow foaming method |
abstract | The invention discloses a method and device for preparing nano metal sulfide powder by using a continuous flow foaming method. A metal sulfide has a general formula of MS, wherein M is selected from divalent ions of Cd, Cu, Mn, Pb or Zn. The method comprises the following steps of: preparing a foaming agent-foam stabilizing agent solution, wherein the concentration of a foaming agent is 0.1-5wt percent, the weight ratio of the foaming agent to a foam stabilizing agent is (6-200):1; dividing the foaming agent-foam stabilizing agent solution into two parts, namely a solution A and a solution B; adding a soluble salt of M into the solution A to ensure that the molar concentration is 0.001-0.5mol/L, stirring to obtain a homogeneous phase solution C; adding a soluble sulfide into the solution B, stirring to obtain a homogeneous phase solution D, wherein the mole number of S<2-> in the solution D is equal to that of M <2+> in the solution C; and introducing gas to ensure that the solution C and the solution D are completely foamed, then mixing, reacting for 2-24h at a constant temperature of 50-100 DEG C, and post-treating to obtain the nano metal sulfide powder. The nano metal sulfide powder prepared by adopting the method is good in dispersibility and uniform in size within a range of 8-50nm, is homogeneous phase without impurities, can be massively prepared and is suitable for industrial production; and the process flow is simple. |
priorityDate | 2012-09-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 83.