http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102964272-B
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_089d40759d5e23b2760341e8f5fd5ce8 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C263-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C265-14 |
filingDate | 2012-11-09-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2014-06-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8d5b81ae910f18f7acd61fbe3841d4e4 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_9d0c04a0d2f2c1934181ffd7216dcd85 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b23624db79cf00868fbe73d8c08c9645 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0481fe172ffe7c3c9c615b8b6e220331 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5af86f9eee46e39856a3b2596fca0022 |
publicationDate | 2014-06-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-102964272-B |
titleOfInvention | Method for preparing hexamethylene-1,6-diisocyanate (HDI) by heterocatalytic pyrolysis in liquid phase |
abstract | The invention belongs to the technical field of organic chemical engineering, and relates to a method for preparing hexamethylene-1,6-diisocyanate (HDI) by heterocatalytic pyrolysis in a liquid phase. A low-boiling solvent and a supported solid catalyst are adopted, the reaction temperature is 180-250 DEG C, the pressure is kept at 0.2-2 MPa, and alkyl alcohol generated by the reaction is transferred out of the system along with nitrogen. The conversion rate of the hexamethylene diamino acid ester is higher than 96%, and the product yield is up to higher than 88%. The invention is simple to operate, and has the advantages of high production safety and reliability, and no environment pollution; and the catalyst and solvent can be easily separated from the product, thereby having high recycling performance. |
priorityDate | 2012-11-09-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 92.