http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102952026-B
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_d42d445a771ee30222eddbe900c23c70 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C213-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F7-18 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C215-28 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C205-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C201-12 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J31-02 |
filingDate | 2012-09-02-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2013-12-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_054e6b39ad977cafd84758244cf1bcb3 |
publicationDate | 2013-12-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-102952026-B |
titleOfInvention | Preparation and synthetic method for chirality (S)-benzene ammonia alcohol hydrochloride |
abstract | The invention discloses a novel chirality (S)-benzene ammonia alcohol hydrochloride. A chemical formula of the S-benzene ammonia alcohol hydrochloride is formed by the following synthetic steps of: carrying out a reaction on N-(2-cyanoethyl)-N-(2-ethoxyl) aniline, (S)-D-phenylglycinol and chromium chloride hexahydrate at the ratio of 1:4.2:1.5 in chlorobenzene solution for 1 day; and standing the reaction liquid for 3 days to obtain the product of chirality clear crystal (S)-benzene ammonia alcohol hydrochloride. The compound has good catalysis performance in nitrile silicide reaction and henry reaction of benzaldehyde, and the yield is respectively up to 77.5 percent and 99.2 percent. |
priorityDate | 2012-09-02-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 49.