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filingDate 2012-10-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2014-09-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b79d9a432b816aa1ee28574718fd1d7c
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publicationDate 2014-09-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-102942460-B
titleOfInvention Unsaturated acetal preparation method
abstract The present invention discloses an unsaturated acetal preparation method. According to the preparation method, an unsaturated alcohol and an unsaturated aldehyde are subjected to a reaction in a pre-reactor to achieve a thermodynamic equilibrium, and then enter a tower type reactor, a water carrying agent is subjected to gasification through a gas generator, and then is subjected to reverse contact with a reaction liquid, and the water generated from the reaction is removed, such that the unsaturated alcohol and the unsaturated aldehyde are subjected to a continuous condensation reaction to prepare the unsaturated acetal. The preparation method has the following characteristics that: the method can be performed under a normal pressure condition, the reaction temperature is constant, low cost synthesis of the unsaturated acetal can be achieved, particularly 3-methyl-2-buten-1-ol and 3-methyl-2-butenal can be adopted as raw materials to synthesize 3-methyl-2-butenal-1 diisopentenyl acetal, wherein the compound is an important intermediate of a synthetic perfume citral.
priorityDate 2012-10-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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