http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102942460-B
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_a564398aa8189633f788e7614fda4876 http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_b992e5f7a0ebce9c8b6dff49206f2764 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C43-303 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C41-56 |
filingDate | 2012-10-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2014-09-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b79d9a432b816aa1ee28574718fd1d7c http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_df016ba24a27a254393a39a5363a54b4 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f6431d0ded5cbe9e4d6a4e415981c2fa http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_36fd6d7b6bb06dfa9b62b7245efb04f5 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8262b97a1254731deef45c922c0caafa http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_71ee7e4e9b8232f972b1ebcd0bdbcc27 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_17e6fce1bdc5822fc13dfdd45c573d4e http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6b2c754cb112fd4c7e887306763a5ec4 |
publicationDate | 2014-09-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-102942460-B |
titleOfInvention | Unsaturated acetal preparation method |
abstract | The present invention discloses an unsaturated acetal preparation method. According to the preparation method, an unsaturated alcohol and an unsaturated aldehyde are subjected to a reaction in a pre-reactor to achieve a thermodynamic equilibrium, and then enter a tower type reactor, a water carrying agent is subjected to gasification through a gas generator, and then is subjected to reverse contact with a reaction liquid, and the water generated from the reaction is removed, such that the unsaturated alcohol and the unsaturated aldehyde are subjected to a continuous condensation reaction to prepare the unsaturated acetal. The preparation method has the following characteristics that: the method can be performed under a normal pressure condition, the reaction temperature is constant, low cost synthesis of the unsaturated acetal can be achieved, particularly 3-methyl-2-buten-1-ol and 3-methyl-2-butenal can be adopted as raw materials to synthesize 3-methyl-2-butenal-1 diisopentenyl acetal, wherein the compound is an important intermediate of a synthetic perfume citral. |
priorityDate | 2012-10-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 58.