http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102911191-B
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_c6fb71722df102c14da56d32f58d79bf |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A61P31-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F1-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F15-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F15-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A61P1-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F3-06 |
filingDate | 2012-10-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2015-05-06-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_63e2877f3cbe52b41daea59dbfacd1cd http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_1b2f087231c01f08fe6bd2c9a12cb3fc http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_597fd37d6b6a5dbce4bd7f8db8199113 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_eca48d6ce6454a94f1c6b42b64d61d51 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_980586b9c9c4a20c38f48941900e4845 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0bcb0029e270d4dbb950cd052e03697b http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4da9659f4d26231a6f2d7513a0fb079e http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4eed5dddceab594311f9544e1e72ecce |
publicationDate | 2015-05-06-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-102911191-B |
titleOfInvention | Preparation method for ethanol 2-hydroxyl naphthaldehyde thiosemicarbazone o-phenanthroline metal complex |
abstract | The invention discloses a preparation method for an ethanol 2-hydroxyl naphthaldehyde thiosemicarbazone o-phenanthroline metal complex, and belongs to the field of bioinorganic chemistry. M is Cu, Zn, Ni or Co. The preparation method comprises the steps of: dissolving thiosemicarbazide in a hot ethanol/water mixed solvent, and carrying out heating and reflowing reaction an ethanol/water solution of 2-hydroxyl naphthaldehyde under a stirring action to obtain 2-hydroxyl naphthaldehyde thiosemicarbazone (H2L); and dissolving the 2-hydroxyl naphthaldehyde thiosemicarbazone (H2L) in a hot ethanol/water mixed solvent, adding an absolute ethanol solution of acetate under the stirring action, dropwise adding an absolute ethanol solution of 1,10-phenanthroline (o-phenanthroline) at the same time, carrying out stirring and heating reaction, cooling and filtering to separate out a solid, namely the ethanol 2-hydroxyl naphthaldehyde thiosemicarbazone o-phenanthroline metal complex. Raw materials are easily available and cheap, and the preparation method is simple and easy to implement and is convenient for industrial production. |
priorityDate | 2012-10-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
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