http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102875591-B

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filingDate 2012-09-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2015-03-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_190f06346a02d29d9fb9999b9c1c0cdf
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publicationDate 2015-03-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-102875591-B
titleOfInvention Method for preparing tetra-tert-butyl orthotitanate composite
abstract The invention discloses a method for preparing a tetra-tert-butyl orthotitanate composite, and relates to a catalyst for preparing room temperature vulcanized silicone rubber (RTV). The method comprises the following steps of: adding 1 molar part of tetraisopropyl titanate and 0 to 0.2 molar part of low-grade glycol into a reaction kettle, stirring at the temperature of between 60 and 70 DEG C, reacting for 0.5 to 1 hour, and distilling a low-boiling substance out under negative pressure; adding 4 to 10 molar parts of tertiary butanol accumulatively for three times into the reaction kettle containing the tetraisopropyl titanate and the low-grade glycol; after adding the tertiary butanol every time, stirring at the temperature of between 60 and 70 DEG C, and reacting for 2 to 2.5 hours; and distilling the low-boiling substance out under the negative pressure to form the tetra-tert-butyl orthotitanate composite. According to the method, the preparation process is easy; and the prepared tetra-tert-butyl orthotitanate composite is stable in quality and can be used as the catalyst for transparent demethanol RTV.
priorityDate 2012-09-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 38.