http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102875270-B
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_16912b3d53aa5055f0a289da7293dbc4 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C211-15 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07B39-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D209-16 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C209-74 |
filingDate | 2012-09-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2014-12-03-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8e46314a1f6545930510ff73a106e24c http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_938292da4e661931df0bdb504aaecc6d http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_63a4faf94479472c63ee7420fbcd7452 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b89d5e4e8ab3573326c417424ef08877 |
publicationDate | 2014-12-03-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-102875270-B |
titleOfInvention | Method for synthesizing trifluoromethyl amine |
abstract | The invention discloses a method for synthesizing trifluoromethyl amine. The method comprises the following steps of: mixing amino acid, anhydrous hydrofluoric acid and sulfur tetrafluoride in a molar ratio of 1:(3-20):(1.8-3.2), and reacting at temperature of between 50 and 150 DEG C for 2 to 10 hours; and cooling, neutralizing, extracting and rectifying to obtain a trifluoromethyl amine product. According to the method, a process is short; and the product is easy to separate, high in yield and stable in quality, the highest yield is 88 percent, and the content of the product is over 97.5 percent. |
priorityDate | 2012-09-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 47.