http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102874871-B
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_9683e667c2fc35e99047b5a77fea519c |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01G39-02 |
filingDate | 2012-10-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2014-07-23-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4a8c2620b62858e8c3f838d1f19a557f http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6913431b75ad88e51d934fb8e29d4c38 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_1be53bc6da9718584adb924c2d47635a http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_608f4a6b4a9e6eae86ab1c4936bff425 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_865ee431bf622447803c53abcfde310a http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_db4cadd8247824e04e65baf05457f20a http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3f30178dfe745131271999e04da67713 |
publicationDate | 2014-07-23-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-102874871-B |
titleOfInvention | Preparation method of molybdenum dioxide core-shell microsphere |
abstract | The invention relates to a preparation method of a molybdenum dioxide core-shell microsphere, and aims to solve the problems that raw materials are difficult to acquire, solvent is an acetophenone reaction system which is not green and environment-friendly and the reaction temperature is high and the reaction time is long in the preparation process in the existing preparation method of a molybdenum dioxide core-shell microsphere. According to the invention, the preparation method of a molybdenum dioxide core-shell microsphere comprises the following steps: 1, mixing molybdenyl acetylacetonate and isopropanol according to a certain ratio to obtain a solution, and dropwisely adding a nitric acid solution into the solution to obtain a mixed solution; and 2, performing heating reaction on the mixed solution obtained in the step 1 to obtain a precursor, flushing the precursor with ethanol, heating, performing vacuum drying, and performing thermal treatment under the atmosphere of nitrogen gas to obtain the molybdenum dioxide core-shell microsphere. The invention can be used in the fields of gas sensitive materials, catalytic materials, chemical adsorption materials, lithium battery materials and the like. |
priorityDate | 2012-10-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 41.