http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102874871-B

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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01G39-02
filingDate 2012-10-26-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2014-07-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4a8c2620b62858e8c3f838d1f19a557f
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publicationDate 2014-07-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-102874871-B
titleOfInvention Preparation method of molybdenum dioxide core-shell microsphere
abstract The invention relates to a preparation method of a molybdenum dioxide core-shell microsphere, and aims to solve the problems that raw materials are difficult to acquire, solvent is an acetophenone reaction system which is not green and environment-friendly and the reaction temperature is high and the reaction time is long in the preparation process in the existing preparation method of a molybdenum dioxide core-shell microsphere. According to the invention, the preparation method of a molybdenum dioxide core-shell microsphere comprises the following steps: 1, mixing molybdenyl acetylacetonate and isopropanol according to a certain ratio to obtain a solution, and dropwisely adding a nitric acid solution into the solution to obtain a mixed solution; and 2, performing heating reaction on the mixed solution obtained in the step 1 to obtain a precursor, flushing the precursor with ethanol, heating, performing vacuum drying, and performing thermal treatment under the atmosphere of nitrogen gas to obtain the molybdenum dioxide core-shell microsphere. The invention can be used in the fields of gas sensitive materials, catalytic materials, chemical adsorption materials, lithium battery materials and the like.
priorityDate 2012-10-26-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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