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publicationDate 2014-09-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-102867954-B
titleOfInvention Method for synthesizing lithium iron phosphate anode material by adopting emulsion liquid phase
abstract The invention discloses a method for synthesizing a lithium iron phosphate anode material by adopting an emulsion liquid phase, belonging to the technical field of chemical material preparation. In the method, by using a water-soluble trivalent iron salt and reduced iron powder as an iron source and phosphoric acid as a phosphorus source as well as lithium hydroxide or lithium carbonate as a lithium source, a lithium iron phosphate precursor is prepared by adopting an emulsion process, and then is dried, subjected to carbon wrapping, and sintered to obtain the lithium iron phosphate anode material. The novel method adopted by the invention ensures that the lithium iron phosphate precursor is generated through reaction in a water phase in a water in oil emulsion, a small-particle-diameter material is easily obtained; meanwhile, all components are easily mixed, all elements are uniformly distributed; and the small-particle-diameter precursor with uniformly distributed components is more beneficial to high-temperature solid phase reaction, thus the sintering time is shortened, and the energy consumption is reduced; and the prepared lithium iron phosphate anode material has excellent electrochemical performance. The method provided by the invention has the characteristics of simple and cheat raw materials, and easy control of a preparation process, and is suitable for large-scale industrialized production.
priorityDate 2012-09-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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