http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102827077-B
Outgoing Links
| Predicate | Object |
|---|---|
| assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_d6a6f422b091ba12ea61d4adbf1b0e8e |
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F9-576 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D221-12 |
| filingDate | 2012-09-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| grantDate | 2014-03-12-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_76c45e274c9585e6da2d424429521f51 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8b199b135ff836c6519e2502a4358e89 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d64c94b01f3d983c0609a5c3e4c25a78 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_adc70817115b5002382e8073c6bcad42 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5588fa1f4ce5da746832599e1ef3271d |
| publicationDate | 2014-03-12-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-102827077-B |
| titleOfInvention | Preparation method for phenanthridine derivative |
| abstract | The invention discloses a preparation method for a phenanthridine derivative. The preparation method comprises the following steps of: adding a catalyst, an oxidant, acid, a 2-phenylaniline compound and an olefin compound into organic solvent; after reaction, carrying out post treatment to obtain the phenanthridine derivative, wherein the catalyst is a bivalent palladium catalyst. According to the preparation method for the phenanthridine derivative disclosed by the invention, the adoption of reagents with high toxicity and high corrosiveness is avoided. The preparation method has the advantages of environment friendliness, easiness in operation, higher yield and simplicity and convenience in post treatment. In addition, a substrate obtained by the method is strong in designability and can be used for designing to synthesize a compound with the required structure according to actual requirements, and thus stronger practicability is realized. |
| priorityDate | 2012-09-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 41.