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filingDate 2012-10-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2014-09-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8c77667c558cbf95829e4cabf4f498c2
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publicationDate 2014-09-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-102826956-B
titleOfInvention Method for separating methyl propionate-methanol-water system by integration of salt-effect extraction and rectification
abstract The invention relates to a method for separating a methyl propionate-methanol-water system by integration of salt-effect extraction and rectification, which comprises the following steps: carrying out salt-effect extraction on a methyl propionate-methanol-water system by using saturated brine as an extractant; after the extraction separation, sending the water phase on the tower bottom of an extraction tower T1 to a methanol recovery tower T3, obtaining methanol of which the mass percent is higher than 99.98% from the T3 tower top and a salt concentrated solution from the T3 tower bottom, and returning the concentrated solution to the extraction tower T1 to be mixed with the extractant for cyclic use; and sending the organic phase from the tower top of the extraction tower T1 to a methyl propionate concentrating tower T2 for further methyl propionate concentration, obtaining a mixture of methyl propionate, methanol and water from the T2 tower top, sending the mixture to the extraction tower T2 to be mixed with the raw material solution for re-extraction, and obtaining methyl propionate of which the mass percent is higher than 99.97% from the T2 tower bottom, wherein the total yield is up to more than 89%. The invention has the advantages of simple technique, high separation efficiency, low production cost, environment friendliness, basically no discharge in the whole process, and the like.
priorityDate 2012-10-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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