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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C309-66
filingDate 2011-03-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2015-03-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6940dd0bdef5ec5634bed2dcd85de817
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a732b0163a0bfe258467590daaee158e
publicationDate 2015-03-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-102791680-B
titleOfInvention Process for preparation of alkyl methanesulfonate solution
abstract A heat-stable solution of an alkyl methanesulfonate in an aromatic organic solvent can be prepared by: reacting an alkyl alcohol with methanesulfonyl chloride in an aromatic organic solvent in the presence of a tertiary amine; and then subjecting the obtained solution of a crude alkyl methanesulfonate in the aromatic organic solvent to washing with an aqueous alkali metal carbonate solution. The washing is conducted using an aqueous alkali metal carbonate solution having a concentration of 1 to 3% by mass in an amount of 4 to 6 parts by mass per part by mass of the alkyl alcohol.
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