http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102775301-B
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_3966ddee295e08cc6fcce4695c77f91b |
classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/Y02P20-50 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C69-50 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C69-44 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C69-40 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C69-48 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C69-42 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J29-40 |
filingDate | 2012-08-06-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2015-07-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_9af2e5744e6ee02bacc749e347acfdef http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a18a5dd79abafe0bd3123a63a64c3a38 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_ef3c90e2b141299a6e42be6a67f47a16 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_c4f30b7bdace761378cf5f61a4b6bedc http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_62db3a7be41632761bb09091a34b94e2 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_887bf991b0574ceb3e45df34f1f229dd http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_16d8c0c03373191c7e9f86959a215a23 |
publicationDate | 2015-07-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-102775301-B |
titleOfInvention | Method for synthesizing aliphatic dibasic acid alkoxy ethyl ester by using ZSM-5 molecular sieve to catalyze |
abstract | The invention provides a method for synthesizing aliphatic dibasic acid alkoxy ethyl ester by using a ZSM-5 molecular sieve to catalyze. The aliphatic dibasic acid and dibasic alcohol ether which are used as raw materials are directly subjected to esterification reaction to synthesize aliphatic dibasic acid alkoxy ethyl ester under the action of the ZSM-5 molecular sieve catalyst and the n-butyl ether azeotropic dehydrating agent; the mass percent of the ZSM-5 molecular sieve catalyst is 0.5-3% of the total mass of reactants; the molar ratio of the dibasic alcohol ether and the aliphatic dibasic acid which the materials reacting to synthesize the aliphatic dibasic acid alkoxy ethyl ester is 2.0:1 to 3.0:1; the reaction temperature is 150-240 DEG C; and the mass percent of the n-butyl ether azeotropic dehydrating agent is 5-30%. The ZSM-5 molecular sieve catalyst and the n-butyl ether azeotropic dehydrating agent are adopted to prepare the aliphatic dibasic acid alkoxy ethyl ester. The process can not cause corrosion to the equipment, causes less pollution to the environment and boasts of economical reaction. The product which is the aliphatic dibasic acid alkoxy ethyl ester is the low-toxicity cold-resistant plasticizer with excellent performance. |
priorityDate | 2012-08-06-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 76.