http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102766160-B
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F9-38 |
filingDate | 2012-07-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2015-09-02-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2015-09-02-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-102766160-B |
titleOfInvention | The novel process of preparing glyphosate by glycin method |
abstract | The present invention relates to the novel process of preparing glyphosate by glycin method, comprise the following steps: glycine, polyoxymethylene, under the effect of catalyzer KOH, addition reaction occur, generate N, N-dihydroxymethyl glycine, solvent is methyl alcohol; N, N-dihydroxymethyl glycine and dimethylphosphite polymerization reaction take place, generate glyphosate methyl esters; Thereafter add hydrochloric acid in reaction solution and carry out acidolysis, generate glyphosate and methylal; Then the de-acidic methanol of distillation, at 115 DEG C, decompression depickling, last suction filtration crystallization, solid is glyphosate, and mother liquor is sodium chloride-containing not, and major ingredient is glyphosate and glyphosate potassium, can do Potassium Fertilizer, pollution-free; Shorten process cycle, reduce manpower and materials and drop into, increase economic efficiency, energy-conserving and environment-protective. |
priorityDate | 2012-07-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 34.