http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102757409-B
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_af1c2f2a9c837a88282f59a7adedee28 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D301-30 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D303-16 |
filingDate | 2012-07-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2014-07-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_be2e6a0ed4e6c4f8358b7dafcf1a4b11 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2056cc850e11c5ae54179a6dbc1e6fe5 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_98afd8ad98a2e2a38da1c740cc2a660b http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2b9990770e09a444f85c6aa8db1436cd |
publicationDate | 2014-07-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-102757409-B |
titleOfInvention | Preparation method of glycidyl acrylate |
abstract | The invention discloses a preparation method of glycidyl acrylate. According to the preparation method, the reactants are acrylic acid and epoxy chloropropane, the catalyst is triethylamine, and the polymerization inhibitor is p-hydroxyanisole. The preparation method comprises the following steps: mixing the polymerization inhibitor, catalyst and reactants, dispersing, and heating to react, wherein under the action of the p-hydroxyanisole, the epoxy chloropropane and triethylamine are subjected to nucleophilic substitution reaction to generate ammonium chloride, and the acrylic acid and carbon positive cations in the ammonium chloride are subjected to esterification reaction to generate the glycidyl acrylate. The product conversion rate is high, however, the production technique consumes fewer raw materials, the operational process is simple and does not need after treatment, and thus, the invention has high economic benefit and social benefit. |
priorityDate | 2012-07-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 33.