http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102746120-A

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_821346e525b6bf2bcc0b5801b5e06e34
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filingDate 2012-06-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f6dba298d02d3480e3c524af562365f6
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_9299b17d170a03e04cff8dcdfb0e8ac3
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publicationDate 2012-10-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-102746120-A
titleOfInvention The synthetic method of cinnamyl alcohol derivative
abstract The invention provides a synthesis method of cinnamyl alcohol derivatives, using benzaldehyde derivatives and β-bromoethanol as raw materials, using triphenylphosphine and an organic base under microwave irradiation, using supercritical carbon dioxide, water, poly The two-phase system formed by ethylene glycol is used as a solvent for the reaction to obtain the cinnamyl alcohol derivative. The invention has mild conditions and can control side reactions to the minimum; it is beneficial to environmental protection, and the waste produced is less and easy to handle; the production process is simplified, the production cost and production cycle are reduced, and it is simple and easy to implement under industrial production conditions. The yield is high, the yield is above 90%, and it is easy to realize industrialized mass production. The cinnamyl alcohol derivatives prepared by the present invention are cinnamyl alcohol derivatives with alkyl substituents on the benzene ring, which are uncommon under natural conditions, fully make up for this natural deficiency, and provide a Synthetic methods of most cinnamyl alcohol derivatives.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-105439818-A
priorityDate 2012-06-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 25.