http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102730770-B

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filingDate 2012-06-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2014-09-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_fbae8b1fd6920c751cdd146df06d3ce4
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publicationDate 2014-09-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-102730770-B
titleOfInvention Preparation method of spongy porous composite oxide nanoscale or microscale polyhedrons
abstract The invention relates to a preparation method of spongy porous composite oxide nanoscale or microscale polyhedrons. The preparation method concretely comprises the following steps: carrying out guiding oxidation and a crystallization reaction on transition metal nitrates which are adopted as raw materials and oxidants with a saccharide as a structure indicator and a reductant, wherein the ratio of the saccharide to the nitrates is 0.5-6; carrying a stirring oxidation reaction under conditions comprising that the pressure is normal pressure and the temperature is 50-95DEG C to obtain a greenish yellow precipitate, and concentrating, washing and filtering the precipitate to obtain a greenish yellow predecessor; and carrying out heat treatment on the predecessor to obtain the spongy porous composite oxide nanoscale or microscale polyhedrons. The method has the advantages of simple operation, low equipment requirements, low cost, high efficiency and easy popularization; and the synthesized polyhedrons have the characteristics of high specific surface area, grading mesopore mode, adjustable dimension, composition, morphology, construction (the specific surface and the aperture distribution) and crystallization degree, and the like, and will be widely applied to the adsorption field, the catalytic field, the magnetic storage field, the magnetic fluid field, the targeting drug carrier field, the cell separation field, the biological medicine field and the like.
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