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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D213-89
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grantDate 2013-12-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2013-12-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-102702094-B
titleOfInvention Synthesis method of copper pyrithione
abstract The invention relates to a synthesis method of copper pyrithione, which is characterized by comprising the following steps: (1) 2-chloropyridine oxidization: adding 2-chloropyridine and a catalyst into a container, and dropwisely adding hydrogen peroxide; (2) filtering the solution obtained in the step (1), carrying out vacuum drying on the filter cake, washing the filter cake, and carrying out vacuum drying on the filter cake again, wherein the obtained filter cake is the catalyst used in the step (1), and the filtrate is a 2-chloropyridine oxynitride solution; and (3) preparation of copper pyrithione. By using the synthesis method provided by the invention, the oxidization yield of 2-chloropyridine is enhanced from 80% to 98%, the total yield is enhanced from 75% to 93%, the product quality is enhanced from 95-96% to more than 98%, and the recycled catalyst can be used repeatedly; and thus, the raw material consumption is reduced, the production cost is lowered, the technological operation is simple, and the wastewater amount and COD (chemical oxygen demand) are obviously reduced.
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type http://data.epo.org/linked-data/def/patent/Publication

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