http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102671657-B

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_45cc3acf07db6fc61114a9c9210563dd
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C303-22
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J23-44
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C309-48
filingDate 2012-03-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2014-06-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4e6c2317141f8703ef7716c0d182e1e8
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_dd34bf3543f231b3a586d11d883db26e
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publicationDate 2014-06-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-102671657-B
titleOfInvention 6-chloro-3-nitrotolyl-4-sulfonic acid liquid-phase hydrogenation catalyst and preparation method thereof
abstract The invention relates to a 6-chloro-3-nitrotolyl-4-sulfonic acid liquid-phase hydrogenation catalyst and a preparation method thereof. The 6-chloro-3-nitrotolyl-4-sulfonic acid liquid-phase hydrogenation catalyst is characterized by comprising 0.05-0.5 wt% of alumina support and the balance of active component metal palladium supported on the alumina support; the metal palladium is distributed on the alumina support surface in an eggshell mode; the specific area of the catalyst is 100-240m<2>/g; and the pore volume of the alumina support is 0.5-0.9ml/g, and the specific area is 100-240m<2>/g. The preparation method comprises the following steps: after oxidizing, roasting and reducing raw materials under certain conditions, drying to obtain the finished catalyst product. The through selectivity of the catalyst is up to more than 96%, the specific productivity is up to 430, and the selectivity is up to more than 96%; and the supported amount of the noble metal palladium can be down to 0.2%, thereby well solving the problem of the relationship between the manufacturing cost and the catalyst performance.
priorityDate 2012-03-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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