http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102660130-B
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_f1fc392ac2ef9a95d94ee2294bec0bb8 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C09B3-30 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/D06P3-62 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/D06P1-24 |
filingDate | 2012-04-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2014-05-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_98d063d7a3b16eaf20942909ebaf77c5 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4b75ec78098030181c6e5fcb110ff5cd http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b2080bee392e517ccaf51f28e57d0525 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4578e844af71cf96fd4d0eb49d9e3922 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_557aecd2ff8e68a6be8146a8ea0431d7 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b87984a8f2b7478faab0d4a6252accdc http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2407b262b43f229bb7ecf1354ff2905c http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0e86d7024f76afe2adbd0a5ef0d399a6 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_95794207024073d032873d486c328183 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_c64aa8d5cb539b3bfa6545c1699fd481 |
publicationDate | 2014-05-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-102660130-B |
titleOfInvention | Method for producing reductive direct black BCN raw dye |
abstract | A method for producing reductive direct black BCN raw dye comprises the following steps: a. brominating BO (bromine) in a non-organic solvent and a non-inorganic acid to obtain purple anthrone bromide; b. performing solid phase reaction, and performing condensation reaction on the purple anthrone bromide and 1-amino anthraquinone under the action of a catalyst and an acid binding agent to obtain a crude reductive direct black BCN dye; and c. acidifying the crude reductive direct black BCN dye and removing impurities to obtain the reductive direct black BCN raw dye. The method has the advantages as follows: firstly, in the BO brominating process, any organic solvent or any inorganic acid is not used, only an oxidant is added into water, and the bromination speed is high; secondly, the condensation reaction does not need any solvent and can be finished by heating in a solid phase container, so that the condensation reaction is very safe and environment-friendly; and thirdly, after the crude dye is acidified and copper is removed, the heavy metal content meets an ETAD requirement. |
priorityDate | 2012-04-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
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