http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102603948-B

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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F126-06
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filingDate 2012-03-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2014-09-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b3686f8af37e0472d5d2712f4b9411da
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publicationDate 2014-09-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-102603948-B
titleOfInvention Polyvinyl pyridine preparing method
abstract The invention relates to a high-yield controllable polyvinyl pyridine synthetic method at room temperature, which includes the steps: firstly, configuration of a reaction system, wherein the reaction system comprises polyvinyl pyridine monomer, initiator, a catalyzing system and solvent, the mole ratio of the polyvinyl pyridine monomer, the initiator and the catalyzing system is 100-1000:1:1, and the mole ratio of the monomer to the solvent is 1:0.5-3; and secondly, preparation of polyvinyl pyridine by 'activity'/ controllable free radical polymerization reaction at 20-30 DEG C. The polyvinyl pyridine polymer is successfully synthetized at the room temperature for the first time by the method, the yield can reach more than 90%, and the precision structure of copolymerized compound is successfully regulated. Further, the polymerization system can be operated without ligand, less zero-valent copper powder is used as catalyst, post-treatment is convenient, and industrial production is facilitated.
priorityDate 2012-03-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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