http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102534718-B

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filingDate 2012-01-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2015-05-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_152e4b548bca6afc51983a6c39204508
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publicationDate 2015-05-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-102534718-B
titleOfInvention Method for preparing PbO2-modified TiO2 nanotube electrode
abstract The invention discloses a method for preparing a PbO2-modified TiO2 nanotube electrode. The method comprises the following steps of: (1) preparing a TiO2 nanotube electrode on a Ti substrate by adopting an anodic oxidation method; (2) depositing PbO2 on the other face of the TiO2 nanotube electrode by using an electrodeposition method at the external voltage of 1.5 V through taking a solution of Pb(NO3)2 and NaF as an electrolyte, wherein the pH value of the solution is 2, the concentration of the Pb(NO3)2 is 0.05 mol/L, and the concentration of the NaF is 0.001 mol/L; (3) naturally airing to obtain a PbO2-TiO2 nanotube/Ti/TiO2 nanotube bifunctional electrode; and (4) obtaining PbO2 bifunctional electrodes with different thicknesses and structures through controlling the current density and the time for deposition. According to the method, the backlight face of the TiO2 nanotube electrode is sufficiently utilized, and the photoelectrocatalytic oxidation capacity of the electrode can be remarkably improved through combining the photocatalysis with the electrocatalysis.
priorityDate 2012-01-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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