http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102531856-B
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_76860418b52f9c22202206cbdf960a27 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C47-575 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C43-275 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C41-01 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C43-263 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C255-50 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C205-38 |
filingDate | 2011-12-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2013-11-13-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5514dfd48bac272236e57fba47394be4 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_630526169a001d3fc244212d57d37d52 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_9393a2c936ada9914a77a01e9933825a http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_95b875a9b14e1843b594368c5a3de6e0 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5db7d6cb1fa2c248a0acac67461eb0f2 |
publicationDate | 2013-11-13-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-102531856-B |
titleOfInvention | Method for synthesizing asymmetric diaryl ether derivative |
abstract | The invention discloses a method for synthesizing asymmetric diaryl ether derivative with a structure shown in a structural formula (I), comprising the following steps: making arylboronic acid and nitrobenzene compound which are raw materials to fully react in an inert organic solvent in the presence of a copper catalyst, an additive and an alkaline compound at 30-150 DEG C, wherein the arylboronic acid has the structural formula (II), and the nitrobenzene compound has the structural formula (III); and postprocessing, separating and purifying a reaction solution after the reaction finishes to obtain the asymmetric diaryl ether derivative. The method for synthesizing the asymmetric diaryl ether derivative has the advantages of mild reaction condition, high reaction yield, good selectivity and low-cost generation cost. |
priorityDate | 2011-12-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 99.