http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102500284-B

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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C251-38
filingDate 2011-11-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2013-12-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3fccd13df1fcef890493bc6fc1bdaa86
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publicationDate 2013-12-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-102500284-B
titleOfInvention Device and method for preparing acetoxime
abstract The invention belongs to the technical field of chemical industry and relates to a device and a method for preparing acetoxime. The acetoxime is prepared from acetone, tertiary butanol, water, ammonia water and hydrogen peroxide by using an integrated TS-1 molecular sieve as a catalyst (an integrated titanium silicalite molecular sieve serves as a catalyst) and through liquid solid phase acetone ammoxidation. The device comprises a condenser, an integrated reactor and an external circulation pump. The integrated TS-1 catalyst (the integrated titanium silicalite molecular sieve serves as the catalyst) synthesized by using frustum-shaped cordierite as a carrier is loaded in the integrated reactor and is applied to preparation of the acetoxime. By adoption of the frustum-shaped cordierite carrier in the device, the wall flow phenomenon can be effectively avoided, so that activity of the catalyst and catalytic efficiency of the reactor are greatly improved. By the device and the method, the problem that the traditional powdered catalyst is difficult to recycle is solved. The device and the method have a wide market application prospect.
priorityDate 2011-11-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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