http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102432584-B

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filingDate 2011-10-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2013-12-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2013-12-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-102432584-B
titleOfInvention Method for preparing high-purity natural vitamin E monomers by separating mixed tocopherol
abstract The invention discloses a method for preparing high-purity natural vitamin E monomers by separating mixed tocopherol. The method comprises the following steps of: fully dissolving the mixed tocopherol in a mobile phase solvent I so as to obtain a loading solution; adding the loading solution into a reversed-phase chromatographic column; adding a mobile phase solvent II into the chromatographic column; and performing step-by-step collection to obtain effluent I of which the purity of d-alpha-tocopherol is more than or equal to 90 percent, effluent II of which the purity of d-gamma-tocopherol is more than or equal to 90 percent and effluent III of which the purity of d-delta-tocopherol is more than or equal to 85 percent. By the method, the one-time column loading and separation of raw materials can be realized under normal pressure so as to obtain three natural vitamin E monomers. A filler in the chromatographic column can be regenerated, the used solvents can be recovered, the cost is reduced, the method is convenient to operate, and the purity is high.
priorityDate 2011-10-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 39.