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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A23L33-00
filingDate 2011-10-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2013-11-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_cd4fb0931c111cacfc9a03bcab925716
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publicationDate 2013-11-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-102349647-B
titleOfInvention Combination containing lutein ester and preparation method thereof
abstract The invention relates to a combination containing lutein ester and a preparation method thereof. The preparation method comprises the steps of: decreasing the temperature of solution of a marigold extract solvent A to 20-28 DEG C, maintaining the temperature for 0.5-4 hours, decreasing the temperature to 5-18 DEG C, maintaining the temperature for 0.5-4 hours and filtering to obtain a filter cake I; and under the condition of 30-70 DEG C, dissolving the filter cake I in a mixed solvent A, agitating for 0.5-5 hours, decreasing the temperature to 10-28 DEG C, keeping the temperature for 0.5-5 hours, filtering to obtain a filter cake II and conducting subsequent steps, wherein the mixed solvent A is the mixed solvent of methyl acetate, acetic ether, n-propyl acetate or butyl acetate and C1-3 alcohol. By adopting the method provided by the invention, the process is simple and feasible, the industrialization is easy to realize, all operations are conducted at low temperature and the stability of the product is guaranteed. The yield of the obtained product highly reaches more than 25 percent, the content of total esters in the product is more than 70 percent, the content of trans-lutein highly reaches 90-93 percent and the bioactivity of the product during use is greatly improved.
priorityDate 2011-10-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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