http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102302539-B
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_38dbef0291a8b858f67596b9cb581373 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A61P39-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A61P35-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A61K36-48 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D311-36 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A61P9-10 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A61P3-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A61P7-02 |
filingDate | 2010-07-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2014-01-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_02a740803d80feefd02fa9ae1a28001a http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_c08a7d038d2a40b108235f1106c20205 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_236d95ae16c51a949c58b22ac8eb0ec5 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_ad973239f19d7d22e37fea24d82e7c93 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_1c88c3965e2ab0bf62ea37afe804ec7a http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d8ec7a33dd86a6b610b057e8f73c9cea http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_ecdc247d992f8dce04e9f68a92d669b5 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_319952471b37105ec262c63eb011ddac |
publicationDate | 2014-01-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-102302539-B |
titleOfInvention | Method for producing trifolium pratense L. isoflavones |
abstract | The invention relates to a method for producing trifolium pratense L. isoflavones, which is characterized by comprising the following steps of: a, extracting, namely extracting trifolium pratense L. by using methanol; b, filtering, namely standing extract in a storage tank, and filtering to remove slag; c, decolorizing and concentrating, namely decolorizing by using an activated carbon column, concentrating, extracting by using petroleum ether and ethyl acetate respectively, and concentrating to obtain a dry product; d, regulating the ph value, namely dissolving the dry product in NaOH aqueous solution, and controlling the ph value to be between 7 and 9; e, loading to a column, namely loading AB-8 macroporous adsorption resin to the column, eluting by using methanol solution, and evaporating until solution is dried; and f, extracting and crystallizing, namely dissolving the dry product in the NaOH aqueous solution, extracting by using the ethyl acetate, concentrating to reach certain volume, and performing cooling crystallization. An isoflavone product with high purity is obtained through steps of extracting solution and column chromatography solution recycling, two-time extraction, column chromatography and the like; a large quantity of solvent, electricity and heat are saved, and the service cycle of resin is prolonged; and by the process, product quality is improved, and energy consumption is reduced. |
priorityDate | 2010-07-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 60.