http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102070592-B

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classificationCPCAdditional http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/Y02P20-55
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D311-32
filingDate 2011-01-26-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2013-06-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_faafc56e55c21d9dd4df98797d79f8c9
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_e87a9d6d26d5e94cf8d3000862e84c2a
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_faa8239af2bc6a9717092b897b151917
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_83c585f856c990803650f28a6ef4add3
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6c35e0156b64c7b693b9deb73c6aadd5
publicationDate 2013-06-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-102070592-B
titleOfInvention Synthesis method of dihydroquercetin
abstract The invention provides a synthesis method of dihydroquercetin, which mainly solves the problems of high preparation cost and unsuitability for large-scale industrial production of dihydroquercetin by the conventional method. The synthesis method of the dihydroquercetin comprises the following steps of: 1, preparing 2,4,6- trihydroxyacetophenone pyran ether; 2, preparing 3,4-protocatechualdehyde dipyran ether; 3, preparing chalcone; 4, preparing epoxy chalcone; and 5, removing a protective group and closing a loop so as to obtain a dihydroquercetin product, wherein a reaction end point is detected by thin layer chromatography. Raw materials and reagents used in a synthesis process are cheap and readily available, the entire route has high yield and low production cost; and the synthesis method has the characteristics of simple process, mature reaction steps, small using amounts of solvents, little environmental pollution, low requirement on production equipment and suitability for industrial production.
priorityDate 2011-01-26-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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