http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-101602669-A

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_761a899f9c1c0eff405aa63fe86d636d
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C69-732
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-03
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J31-04
filingDate 2009-07-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8136174ded9d99882a1000bfeced7589
publicationDate 2009-12-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-101602669-A
titleOfInvention The oxidation inhibitor triglycol is two-preparation method of [3-(3-tertiary butyl-4-hydroxy-5-aminomethyl phenyl) propionic ester]
abstract The present invention relates to a kind of preparation method of oxidation inhibitor, relate in particular to a kind of preparation method of hindered phenolic oxidation inhibitor.Preparation method provided by the invention is divided into five steps: (1) raw material joins in the reactor and displaces wherein air; (2) heating makes the raw material melting and removes wherein light constituent and water; (3) add the zn cpds catalyzer; (4) 150~200 ℃ were reacted 2~9 hours down, and the methyl alcohol of generation is discharged reactive system; (5) cool to and add acid neutralization below 120 ℃.This method have the reaction times short, reaction solution is of light color, catalyst levels is little and characteristics such as easy removal.1. the product that utilizes this method to make has the purity height, quality is good, can directly apply to the production of derived product; 2. good stability, the long storage nondiscoloration; 3. remaining trace catalyst does not influence product stability energy and application performance.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114805929-A
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-106700129-A
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-106700129-B
priorityDate 2009-07-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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