http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-101575300-B
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_6a201fbfc9902838caa46fbbe2b73ef2 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C231-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C237-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C231-18 |
filingDate | 2009-06-11-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2012-10-03-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f058d5e6615349667547a3b1c9cafa51 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_49b56e1db237f14e191088d6c42b7ed0 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_aa8a58e4178c68a66d3aacf08fbbcdda http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3357cf90035dd507b350148d4f2d9fef |
publicationDate | 2012-10-03-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-101575300-B |
titleOfInvention | The production method of S-2-aminobutanamide |
abstract | The invention discloses a production method of S-2-aminobutyramide, which belongs to the technical field of chemical synthesis. The invention uses L-(+)-methionine as a raw material, and in the presence of alcohol or ether solvents, through chlorine-containing organic Carboxylate effect, demethylation thiohydroxylation and formation of S-2-amino-4-hydroxybutyric acid hydrochloride, followed by hydroxyl bromination to give S-2-amino-4-bromobutyric acid hydrobromide, S-2-amino-4-bromobutyric acid methyl ester hydrochloride is obtained by carboxymethyl esterification, nickel-catalyzed hydrogenation dehalogenation is converted into S-2-aminobutyric acid methyl ester, and finally aminolysis generates S-2-amino Butanamide. The invention has the advantages of high yield and good safety. |
priorityDate | 2009-06-11-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Predicate | Subject |
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isDiscussedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/substance/SID421410965 http://rdf.ncbi.nlm.nih.gov/pubchem/compound/CID7015191 |
Total number of triples: 18.