http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-101157614-A
Outgoing Links
| Predicate | Object |
|---|---|
| assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_fd39612dd1faf2facbc47ee36bf27474 |
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-307 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C69-63 |
| filingDate | 2007-09-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3b749d34594e48747457cb99db00260c http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_141829e66ebf08196d7548a500958997 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_e90a5a29cdc9c67080fb6fcb57c0100c http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4354b0786a888f49c37ef40925260cb4 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2e9befe6dd0c853f1c0ca2c2ca0e73ad http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_624e2eb8f79322eb8317d8e11c195bd9 |
| publicationDate | 2008-04-09-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-101157614-A |
| titleOfInvention | Chemical method for synthesizing 6,8-dichloro ethyl cacodylic acid caprylate |
| abstract | The invention discloses a chemical synthetic method for 6, 8-ethyl octylate chloride. The method comprises the steps as follows: 6-hydroxyl-8-ethyl octylate chloride is dissolved in N, N-dimethylformamide; solution which is dissolved with organic solution of double (trichloride trichloromethyl)-carbonic acid ester is dropped in when in mixing under the cold water bath condition; the solution is gradually warmed to 50 to 90 DEG C for reacting for 2 to 8 hours after dropping; and the reaction solution is disposed into 6, 8-ethyl octylate chloride after finishing the reaction. As the invention replaces sulphoxides chloride with double (trichloride trichloromethyl)-carbonic acid ester, the invention produces environment friendly Vilsmeier agent which needs not to be separated in the reaction, and the Vilsmeier agent directly reacts with 6-hydroxyl-8-ethyl octylate chloride to produce 6, 8-ethyl octylate chloride. Besides, the invention has the advantages of advanced art, rational technological condition, simple and safe operation, high reaction yield, low production cost, low three-waste emission as well as great implementation value and social and economic efficiency. |
| isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103232344-B http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103232344-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-105693510-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-106966901-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-106966900-A |
| priorityDate | 2007-09-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 52.