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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01B15-12
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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01B15-023
filingDate 1966-11-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_9d30361d7750f0e0ce62db389979ded3
publicationDate 1973-05-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CH-536792-A
titleOfInvention Process for the preparation of perborates
abstract Organic compound with two available H atoms is oxidised to H2O2 in organic solvent mixture, or H2O2 is added to solvent. 0.1 - 0.6 mole Me2B4O7 per mole H2O2 is added and the mixture is recirculated for e.g. 40 min. at 10 - 60 degrees C. Solid product is filtered off. Me may be alkali metal, e.g. Na. Reaction proceeds by stages; Na2B4O7 right arrow NaB4O7.H2O2 right arrow NaBO2.H2O2 right arrow NaBO2.2H2O2 + NaBO2.H2O2. Purification is by benzene washing and vacuum drying. Method is safe, and avoids loss of active oxygen.
priorityDate 1965-05-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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