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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C67-52
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C69-82
filingDate 1968-12-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_492b9be1e07b5a812b66ea9a8133336a
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_341e0e1940a44b2c1a79ef3bdd46ee9b
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_e92bd5a3973eaa654ab3c24a620a1d0b
publicationDate 1972-08-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CH-526503-A
titleOfInvention Process for the production of bis (B-hydroxyethyl) terephthalate of a high degree of purity
abstract Crude bis(beta-hydroxyethyl) terephthalate (BHET) is purified by (1) dissolving in a hot aromatic solvent to a concentration higher than the saturation solubility of the ester at the apparat melting point (Tm) of BHET in the solvent; the solvent is at a temp. higher than Tm, (2) cooling the solution very rapidly to below Tm so that the precipitate is not granular or lumpy, and (3) separating off the solid. Impurities are removed which retard the polycondensation of the ester and discolour the polymer and lower its melting point. Recrystallisation processes using other solvents, e.g. water (US. 3,062,862) and polar organic solvent (US. 3,120,560 and 3,268,575) are complicated by the high solubility of the ester in these solvents at ambient temp.
priorityDate 1968-12-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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