http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CH-522638-A
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_93ac09b77f237974128330bb530e9baf |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D209-48 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D- http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D243-32 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D209-48 |
filingDate | 1968-08-28-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_01e2cdee37d0315fd79c27cab6081cf5 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6d11b085cbc6b38eb497385573c4879f |
publicationDate | 1972-06-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CH-522638-A |
titleOfInvention | Process for the preparation of 2-phthalimidoacetamido-5-nitrobenzophenone |
abstract | 2-Phthalimidoacetamido-5-nitrobenzophenone (I) Intermediate for the preparation of 7-nitro-5-phenyl-1,4-3H-benzo-diazepine 2 (1H)-one, a powerful sedative with low toxicity. A solution of 4.4 g. phthalimidoacetyl chloride and 4.8 g. 2-amino-5-nitrobenzophenone in 30 ml. methylene chloride is boiled for 1 night under reflux. The crystalline precipitate is filtered off and the filtrate concentrated. The second fraction is combined with the first to give 8.3 g. 2-phthalimidoacetamido-5-nitrobenzophenone, purified by crystallising from methanol, m.p. 205-207 deg.C. |
priorityDate | 1967-09-09-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 34.