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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C273-1827
classificationIPCAdditional http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C275-64
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C273-18
filingDate 1966-10-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_132ce362b139f2ede12d5e1bdb1db7e9
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f7b9be4596577a25bf15a824a83e01eb
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0336d5728a53f9743746c7efd1d8016a
publicationDate 1970-09-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CH-496677-A
titleOfInvention Process for the preparation of N-phenyl-N'-alkoxy-N'-alkylureas
abstract Prodn. of N-phenyl-N'-alkoxy-N'-alkyl ureas (I):- (R')OR Ar = opt. substd. phenyl R' and R = alkyl. (I) are plant protection agents. The first stage of the reaction is carried out using 5-30%, pref. 10-30% aqs. hydroxylamine in the presence of a water immiscible solvent such as benzene, CHCl3 or diethylether. The hydroxyamine is pref. used in excess with respect to the isocyanate. Reaction temps. are in the range of 0-25 deg.C and when the first stage is complete, the organic layer is separated off with the impurities. The second (alkylation) stage is carried out by usual methods e.g. with alkyl sulphates, alkyl halides or alkyl sulphonates.
priorityDate 1965-11-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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