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filingDate 2019-03-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2022-10-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5e298a7229f2505e6f64c2a3a9419909
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publicationDate 2022-10-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CA-3092426-C
titleOfInvention Continuous synthesus of n-alkyl-nitratoethylnitramines at elevated pressures
abstract Provided herein is a process for the continuous synthesis of N-alkyl nitratoethylnitramines. The process may comprise the preparation of a compound of the formula (I): or of mixtures of two or more such compounds, where R is an alkyl group having from 1 to 6 carbon atoms or a group of the formula -CH2-CH2-0-NO2. The process may also comprise the reaction of a compound of the formula (II), or of two or more of such compounds: wherein R' is an alkyl group having from 1 to 6 carbon atoms or a group of the formula -CH2-CH2-0H, with nitric acid and then with a mixture of at least one acid anhydride and a chloride-containing catalyst in a continuous process. The reactions may be carried out at a pressure of from 2 bar above atmospheric pressure up to a pressure of 80 bar above atmospheric pressure.
priorityDate 2018-03-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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