http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CA-2899087-A1

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filingDate 2014-12-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_9104c030cabd842b5c84cd34f5c35544
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publicationDate 2015-06-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CA-2899087-A1
titleOfInvention Process for the preparation of succinic acid ester
abstract A process for the production of dialkyl succinate from a bio-succinic acid feedstock comprising the steps of: feeding bio-succinic acid to a point at or near the bottom of a reaction distillation zone column operated at temperatures and pressures to enable esterification of the succinic acid and passing said stream co-currently with upflowing alkanol such that said esterification reaction occurs: removing an overhead vapour stream from at or near the top of the reaction distillation zone column comprising di-ester, alkanol, water of esterification and organic components and passing said stream to an alkanol separation column where the alkanol is separated from the water of esterification and from the organic components; removing a side draw from the alkanol separation column from a point below the feed point thereto, said side draw comprising partially immiscible organic and aqueous phases; passing said side draw to phase separation apparatus where the partially immiscible organic and aqueous phases are separated; passing said organic phase to a column where the dialkyl succinate is separated from residual water and other organic components; and recovering the dialkyl succinate.
priorityDate 2013-12-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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