http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CA-2023164-C
Outgoing Links
Predicate | Object |
---|---|
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F9-145 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J31-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F9-145 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07B61-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F9-141 |
filingDate | 1990-08-13-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2000-06-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_53a357b2aa2a38244cbcebf847a4c6e4 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_193d72fac23c528436b918a05af03a02 |
publicationDate | 2000-06-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CA-2023164-C |
titleOfInvention | Process for the preparation of tris-(2,4-ditert-butylphenyl)phosphite |
abstract | A process far the preparation of tris-(2,4-ditert-butylphenyl) phosphate from 2,4-ditert-butylphenol and phosphorus trichloride in the presence of catalysts, which comprises carrying out the reaction in an at least three-stage process in which the 2,4-ditert-butylphenol and 40 - 100 % of the catalyst are combined in a preliminary stage and are brought together with the phosphorus trichloride in a first stage, these being allowed to react under normal pressure and at temperatures of 55 to 70°C for a dwell time of 15 to 40 minutes, the reaction mixture is then reacted in a second stage under normal pressure and at temperatures of over 140°C, remaining amounts of catalyst being added to the first and/or second reaction stage, the reaction mixture is then kept under reduced pressure at temperatures of at least 186°C in a third reaction stage, and the tris-(2,4-ditert-butylphenyl) phosphate is then isolated from the reaction mixture, the process being carried out in the absence of solvents. |
priorityDate | 1989-08-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 145.