http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CA-1278143-C

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filingDate 1987-08-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1990-12-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_cb570f7157473390478b2b94e227f666
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8adca4a712c2fd79c938b33a3e57731c
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publicationDate 1990-12-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CA-1278143-C
titleOfInvention Process for producing polyarylene sulfide
abstract ABSTRACT OF THE DISCLOSURE Disclosed herein is a process for producing a medium-or high-molecular-weight polyarylene sulfide which comprises subjecting an alkali metal sulfide, a dihalo aromatic compound and optionally, small amount of tri- or higher polyhalo aromatic compound to dehalogenation and sulfidation reaction at a temperature of from 235 to 280°C in the presence of a water in amount of from 0.5 to 5 mol per 1 kg of an aprotic organic polar solvent until the conversion of said dihalo aromatic compound reaches from 70 to 98 mol%, thereby forming a polyarylene sulfide prepolymer having a melt viscosity of from 5 to 300 poise (as measured at 310°C under a shear rate of 200 sec-1), adding water to the resultant reaction mixture containing the polyarylene sulfide prepolymer so that from 6 to 15 mol of water is present per 1 kg of said solvent, and then continuing the reaction at a temperature of from 240 - 290°C, in which the reaction comprising said two steps is conducted for from 1 to 10 hours. The polyarylene sulfide (PAS) produced the process of the present invention is useful as a material for the production of electronic equipments and automobile parts.
priorityDate 1986-08-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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